@article{oai:tsukuba.repo.nii.ac.jp:00037652, author = {鈴木, 義和 and Maki, Ryosuke S. S. and Morgan, Peter E. D. and Suzuki, Yoshikazu}, issue = {1}, journal = {Powder Diffraction}, month = {Mar}, note = {We have used conventional X-ray powder diffraction to study one of the largest volume inorganic mixed oxide unit-supercell structures done so far. This necessitated some small-angle X-ray scattering-like observations at low angles from <2° 2θ to concord with electron diffraction, which had indicated an 8 × 8 × 8 huge volume supercell of a fluorite-type basic sub-cell. Emphasis is on the detection of, possibly very weak, fingerprint, low-angle/long lines/peaks which will indicate the (often unsuspected) presence of complex polytypic arrangements of simple very strong basic sub-cells and so facilitate future synthetic studies.}, pages = {8--15}, title = {X-ray powder diffraction characterization of the large-volume unit cell of the M8 murataite polytype}, volume = {31}, year = {2016} }