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Ordering Phase Transition with Symmetry-Breaking from Disorder over Non-Equivalent Sites: Calorimetric and Crystallographic Study of Crystalline d-Sorbose
http://hdl.handle.net/2241/00161580
http://hdl.handle.net/2241/001615807ae2fcbb-7cc8-4333-a5ca-48e416961b0c
名前 / ファイル | ライセンス | アクション |
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Crystals_10-5 (1.1 MB)
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Item type | Journal Article(1) | |||||||||||
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公開日 | 2020-10-15 | |||||||||||
タイトル | ||||||||||||
言語 | en | |||||||||||
タイトル | Ordering Phase Transition with Symmetry-Breaking from Disorder over Non-Equivalent Sites: Calorimetric and Crystallographic Study of Crystalline d-Sorbose | |||||||||||
言語 | ||||||||||||
言語 | eng | |||||||||||
資源タイプ | ||||||||||||
資源 | http://purl.org/coar/resource_type/c_6501 | |||||||||||
タイプ | journal article | |||||||||||
著者 |
山村, 泰久
× 山村, 泰久
WEKO
205003
× 菱田, 真史× 齋藤, 一弥× Iwagaki, Sakiko× Kakuta, Hiroki× Saitoh, Hideki× Fukada, Kazuhiro |
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抄録 | ||||||||||||
内容記述タイプ | Abstract | |||||||||||
内容記述 | Phase transitions in the crystalline state of chiral sorbose were examined using precise heat capacity calorimetry and X-ray crystallography. The calorimetry established heat capacity below room temperature. Besides the known transition (main transition) at 199.5 K, the calorimetry detected plural thermal anomalies assignable to new phase transitions (around 210 K) and a glass transition (at ca. 120 K). The X-ray diffraction at low temperatures established the crystal structure of the lowest temperature phase. The identification of the broken symmetry upon the main transition solves an apparent contradiction that the structural disorder reported previously does not contribute seemingly to the symmetrization. | |||||||||||
書誌情報 |
en : Crystals 巻 10, 号 5, p. 361, 発行日 2020-05 |
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ISSN | ||||||||||||
収録物識別子タイプ | ISSN | |||||||||||
収録物識別子 | 2073-4352 | |||||||||||
DOI | ||||||||||||
識別子タイプ | DOI | |||||||||||
関連識別子 | 10.3390/cryst10050361 | |||||||||||
権利 | ||||||||||||
権利情報 | © 2020 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/). | |||||||||||
著者版フラグ | ||||||||||||
値 | publisher | |||||||||||
出版者 | ||||||||||||
出版者 | MDPI |