WEKO3
アイテム
{"_buckets": {"deposit": "4dafaed1-017e-480e-8ea5-46d230ce88e9"}, "_deposit": {"id": "28723", "owners": [], "pid": {"revision_id": 0, "type": "depid", "value": "28723"}, "status": "published"}, "_oai": {"id": "oai:tsukuba.repo.nii.ac.jp:00028723", "sets": ["1944", "2022"]}, "item_5_biblio_info_6": {"attribute_name": "書誌情報", "attribute_value_mlt": [{"bibliographicIssueDates": {"bibliographicIssueDate": "2013-03", "bibliographicIssueDateType": "Issued"}, "bibliographicIssueNumber": "3", "bibliographicPageEnd": "251", "bibliographicPageStart": "244", "bibliographicVolumeNumber": "16", "bibliographic_titles": [{"bibliographic_title": "Comptes rendus. Chimie"}]}]}, "item_5_creator_3": {"attribute_name": "著者別名", "attribute_type": "creator", "attribute_value_mlt": [{"creatorNames": [{"creatorName": "鈴木, 義和"}], "nameIdentifiers": [{"nameIdentifier": "633", "nameIdentifierScheme": "WEKO"}, {"nameIdentifier": "40357281", "nameIdentifierScheme": "e-Rad", "nameIdentifierURI": "https://nrid.nii.ac.jp/ja/nrid/1000040357281"}, {"nameIdentifier": "0000003029", "nameIdentifierScheme": "筑波大学研究者総覧", "nameIdentifierURI": "http://trios.tsukuba.ac.jp/researcher/0000003029"}]}]}, "item_5_description_4": {"attribute_name": "抄録", "attribute_value_mlt": [{"subitem_description": "By using the droplet-fixation method, quantitative analyses of the size and dispersion state of electrosprayed droplets were conducted. At first, titanium(IV) bis (ammonium lactate) dihydroxide (TALH) aqueous solution (2 wt%), as a precursor of TiO2, was electrosprayed using single-nozzle setting, and the electrospray parameters were optimized. Fine and monodispersed droplets (5.00 μm with the geometrical standard deviation of 1.16) were successfully obtained. Then, applying the single-nozzle conditions, we tried to prepare the double-nozzle electrospray, where positively and negatively charged sprays were superimposed to neutralize the charges of droplets. As for the double-nozzle electrospray, relatively fine and monodispersed droplets (7.58 μm with the geometrical standard deviation of 1.37) were obtained. By using the double-nozzle electrospray, the final TiO2 powder yield after pyrolysis can be much improved.", "subitem_description_type": "Abstract"}]}, "item_5_identifier_34": {"attribute_name": "URI", "attribute_value_mlt": [{"subitem_identifier_type": "HDL", "subitem_identifier_uri": "http://hdl.handle.net/2241/118908"}]}, "item_5_publisher_27": {"attribute_name": "出版者", "attribute_value_mlt": [{"subitem_publisher": "Elsevier Masson SAS"}]}, "item_5_relation_11": {"attribute_name": "DOI", "attribute_value_mlt": [{"subitem_relation_type_id": {"subitem_relation_type_id_text": "10.1016/j.crci.2012.11.003", "subitem_relation_type_select": "DOI"}}]}, "item_5_rights_12": {"attribute_name": "権利", "attribute_value_mlt": [{"subitem_rights": "© 2012 Académie des sciences. Published by Elsevier Masson SAS this is the author’s version of a work that was accepted for publication in Materials research bulletin. Changes resulting from the publishing process, such as peer review, editing, corrections, structural formatting, and other quality control mechanisms may not be reflected in this document. Changes may have been made to this work since it was submitted for publication. A definitive version was subsequently published in Comptes Rendus Chimie, VOL16(3) 244–251 2013 DOI:10.1016/j.crci.2012.11.003"}]}, "item_5_select_15": {"attribute_name": "著者版フラグ", "attribute_value_mlt": [{"subitem_select_item": "author"}]}, "item_5_source_id_7": {"attribute_name": "ISSN", "attribute_value_mlt": [{"subitem_source_identifier": "1631-0748", "subitem_source_identifier_type": "ISSN"}]}, "item_5_source_id_9": {"attribute_name": "書誌レコードID", "attribute_value_mlt": [{"subitem_source_identifier": "AA11609870", "subitem_source_identifier_type": "NCID"}]}, "item_5_subject_20": {"attribute_name": "NIIサブジェクト", "attribute_value_mlt": [{"subitem_subject": "基礎工学・応用物理学", "subitem_subject_scheme": "Other"}]}, "item_creator": {"attribute_name": "著者", "attribute_type": "creator", "attribute_value_mlt": [{"creatorNames": [{"creatorName": "Matsubara, Takeo"}], "nameIdentifiers": [{"nameIdentifier": "99396", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "Suzuki, Yoshikazu"}], "nameIdentifiers": [{"nameIdentifier": "99397", "nameIdentifierScheme": "WEKO"}]}, {"creatorNames": [{"creatorName": "Tohno, Susumu"}], "nameIdentifiers": [{"nameIdentifier": "99398", "nameIdentifierScheme": "WEKO"}]}]}, "item_files": {"attribute_name": "ファイル情報", "attribute_type": "file", "attribute_value_mlt": [{"accessrole": "open_date", "date": [{"dateType": "Available", "dateValue": "2013-12-25"}], "displaytype": "detail", "download_preview_message": "", "file_order": 0, "filename": "CRC_16-3.pdf", "filesize": [{"value": "487.7 kB"}], "format": "application/pdf", "future_date_message": "", "is_thumbnail": false, "licensetype": "license_free", "mimetype": "application/pdf", "size": 487700.0, "url": {"label": "CRC_16-3.pdf", "url": "https://tsukuba.repo.nii.ac.jp/record/28723/files/CRC_16-3.pdf"}, "version_id": "d84ee915-6962-4f67-b459-2e55ede825a7"}]}, "item_language": {"attribute_name": "言語", "attribute_value_mlt": [{"subitem_language": "eng"}]}, "item_resource_type": {"attribute_name": "資源タイプ", "attribute_value_mlt": [{"resourcetype": "journal article", "resourceuri": "http://purl.org/coar/resource_type/c_6501"}]}, "item_title": "Synthesis and characterization of TiO2 powders by the double-nozzle electrospray pyrolysis method. Part 1. Refinement and monodispersion of sprayed droplets", "item_titles": {"attribute_name": "タイトル", "attribute_value_mlt": [{"subitem_title": "Synthesis and characterization of TiO2 powders by the double-nozzle electrospray pyrolysis method. Part 1. Refinement and monodispersion of sprayed droplets"}]}, "item_type_id": "5", "owner": "1", "path": ["1944", "2022"], "permalink_uri": "http://hdl.handle.net/2241/118908", "pubdate": {"attribute_name": "公開日", "attribute_value": "2013-05-09"}, "publish_date": "2013-05-09", "publish_status": "0", "recid": "28723", "relation": {}, "relation_version_is_last": true, "title": ["Synthesis and characterization of TiO2 powders by the double-nozzle electrospray pyrolysis method. Part 1. Refinement and monodispersion of sprayed droplets"], "weko_shared_id": 5}
Synthesis and characterization of TiO2 powders by the double-nozzle electrospray pyrolysis method. Part 1. Refinement and monodispersion of sprayed droplets
http://hdl.handle.net/2241/118908
http://hdl.handle.net/2241/118908a114696f-5c41-41f1-8cb9-4241b7fc27b1
名前 / ファイル | ライセンス | アクション |
---|---|---|
CRC_16-3.pdf (487.7 kB)
|
|
Item type | Journal Article(1) | |||||
---|---|---|---|---|---|---|
公開日 | 2013-05-09 | |||||
タイトル | ||||||
タイトル | Synthesis and characterization of TiO2 powders by the double-nozzle electrospray pyrolysis method. Part 1. Refinement and monodispersion of sprayed droplets | |||||
言語 | ||||||
言語 | eng | |||||
資源タイプ | ||||||
資源 | http://purl.org/coar/resource_type/c_6501 | |||||
タイプ | journal article | |||||
著者 |
Matsubara, Takeo
× Matsubara, Takeo× Suzuki, Yoshikazu× Tohno, Susumu |
|||||
著者別名 |
鈴木, 義和
× 鈴木, 義和 |
|||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | By using the droplet-fixation method, quantitative analyses of the size and dispersion state of electrosprayed droplets were conducted. At first, titanium(IV) bis (ammonium lactate) dihydroxide (TALH) aqueous solution (2 wt%), as a precursor of TiO2, was electrosprayed using single-nozzle setting, and the electrospray parameters were optimized. Fine and monodispersed droplets (5.00 μm with the geometrical standard deviation of 1.16) were successfully obtained. Then, applying the single-nozzle conditions, we tried to prepare the double-nozzle electrospray, where positively and negatively charged sprays were superimposed to neutralize the charges of droplets. As for the double-nozzle electrospray, relatively fine and monodispersed droplets (7.58 μm with the geometrical standard deviation of 1.37) were obtained. By using the double-nozzle electrospray, the final TiO2 powder yield after pyrolysis can be much improved. | |||||
書誌情報 |
Comptes rendus. Chimie 巻 16, 号 3, p. 244-251, 発行日 2013-03 |
|||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 1631-0748 | |||||
書誌レコードID | ||||||
収録物識別子タイプ | NCID | |||||
収録物識別子 | AA11609870 | |||||
DOI | ||||||
識別子タイプ | DOI | |||||
関連識別子 | 10.1016/j.crci.2012.11.003 | |||||
権利 | ||||||
権利情報 | © 2012 Académie des sciences. Published by Elsevier Masson SAS this is the author’s version of a work that was accepted for publication in Materials research bulletin. Changes resulting from the publishing process, such as peer review, editing, corrections, structural formatting, and other quality control mechanisms may not be reflected in this document. Changes may have been made to this work since it was submitted for publication. A definitive version was subsequently published in Comptes Rendus Chimie, VOL16(3) 244–251 2013 DOI:10.1016/j.crci.2012.11.003 | |||||
著者版フラグ | ||||||
値 | author | |||||
出版者 | ||||||
出版者 | Elsevier Masson SAS | |||||
URI | ||||||
識別子 | http://hdl.handle.net/2241/118908 | |||||
識別子タイプ | HDL |